Instrumental analysis
Informacje ogólne
Kod przedmiotu: | R.4sa.IAS.SM.ROSAY |
Kod Erasmus / ISCED: | (brak danych) / (brak danych) |
Nazwa przedmiotu: | Instrumental analysis |
Jednostka: | Wydział Rolniczo-Ekonomiczny |
Grupy: | |
Punkty ECTS i inne: |
(brak)
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Język prowadzenia: | angielski |
Skrócony opis: |
Scientific basis and construction principles of analytical instruments as well as their functioning and usability in agricultural and environmental research according to chosen electrochemical, titrimetric, spectroscopic and chromatographic methods. In practicals, the students will work with different modern analytical equipment, measuring and assessing of accuracy, precision and detection limit of selected methods for determining of some elements in environmental materials |
Pełny opis: |
Lectures (5 x 2 hours) 1. Classification of instrumental methods and preparation of samples for analysis. 2. Incineration and wet mineralization of samples. 3. Atomic Absorption Spectroscopy (AAS). 4. Atomic Emission Spectroscopy – Plasma Emission Spectroscopy (ICP-OES). 5. Chromatography and errors in the sample analysis. Lab practicals (5 x 3 hours) 1. Preparation and dissolving samples of soil and plant material before analysis. 2. Operation of UV-VIS Spectrophotometer (Beckman DU600) and its application for environmental material analyses. 3. Operation of Atomic Absorption Spectrometer (Solaar M6) and its application for environmental material analyses. 4. Operation of Atomic Emission Spectrometer (ICP-OES – Jobin-Yvon 238 ULTRACE) and its application for environmental material analyses. 5. Hydraulic conductivity measurement. Subject statistic 1.. Number of hours and ECTS credits - compulsory subject Hours: 75; ECTS: 3 2. Number of hours and ECTS credits - facultative subject Hours: -; ECTS: - 3. Total number of hours and ECTS credits, a student must earn by direct contact with academics (lectures, classes, seminars....) Hours: 25; ECTS: 1,0 4. Total number of hours and ECTS credits, a student earns in the course of a practical nature, such as laboratory, field trips and design classes Hours: 15; ECTS: 0,6 5. Expected personal workload (without or with academics participation during consultations) necessary for realization of subject objectives. Hours: 50; ECTS: 2,0 |
Literatura: |
Kim H. Tan: Soil Sampling, Preparation, and Analysis – Second Edition, Marcel Dekker, Inc., New York, USA, ss. 408. Kim H. Tan: Soil Sampling, Preparation, and Analysis. CRC Press Taylor and Francis Group LLC, Boca Raton, USA, ss. 623. |
Efekty uczenia się: |
Knowledge - student possesses knowledge about collecting, preparation and analysis of samples using methods applied in agricultural and environmental laboratories Skills - student is able to plan and conduct analysis of various samples - understands the need and estimates analytical error values Social competences - organizes analytical work in a small team - is aware of necessary constant monitoring of the analytical work quality |
Metody i kryteria oceniania: |
Formative grades (practicals) 1. Assessment of student activity and involvement in analytical work (30% of final grade) 2. Written and oral tests on the principles and potential applications of cognitive methods and instruments (70% of final grade). Lectures: 1st term – written, time-limited examination (problem solving); 2nd term – oral examination |
Właścicielem praw autorskich jest Uniwersytet Rolniczy im. Hugona Kołłątaja w Krakowie.